(E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

Base Information

Chemical Name:(E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone
CAS No.:1353852-08-0
Molecular Formula:C₂₄H₂₅F₃O₃
Molecular Weight:418.456
Hs Code.:

Synonyms:(E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

Suppliers and Price of (E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

Chemical Property:

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Technology Process of (E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

There total 1 articles about (E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 213971-37-0
3,4-dihydro-6,7-dimethoxy-3-methyl-5-n-propyl-1(2H)naphthalenone

: 1353852-08-0
(E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

Guidance literature:: With potassium hydroxide; In ethanol; water; at 20 ℃;
DOI:10.1016/j.tetlet.2011.11.065

Reference yield:

: 1353852-08-0
(E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

: 1353852-28-4
2-(4-trifluoromethylbenzyl)-6,7-dimethoxy-3-methyl-5-propyltetralone

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 1h; under 1551.49 Torr; Autoclave;
DOI:10.1016/j.tetlet.2011.11.065

Reference yield:

: 1353852-08-0
(E)-2-(4-trifluoromethylbenzylidene)-6,7-dimethoxy-3-methyl-5-propyl-1-tetralone

: 1353852-50-2
3-(4-(trifluoromethyl)benzyl)-1,2-dihydro-6,7-dimethoxy-2-methyl-8-propylnaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C / 1551.49 Torr / Autoclave

2: sodium tetrahydroborate / ethanol / 2 h / Reflux

3: hydrogenchloride / water / 2 h / Reflux

With hydrogenchloride; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; In ethanol; water; ethyl acetate;
DOI:10.1016/j.tetlet.2011.11.065