C₄₁H₅₂N₄O₅

Base Information

Chemical Name:C₄₁H₅₂N₄O₅
CAS No.:1613708-27-2
Molecular Formula:C₄₁H₅₂N₄O₅
Molecular Weight:680.888
Hs Code.:

C<sub>41</sub>H<sub>52</sub>N<sub>4</sub>O<sub>5</sub>

Synonyms:C₄₁H₅₂N₄O₅

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Chemical Property of C₄₁H₅₂N₄O₅

Chemical Property:

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Technology Process of C₄₁H₅₂N₄O₅

There total 18 articles about C₄₁H₅₂N₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613625-69-6
C₃₀H₃₆N₂O₆

: 42817-60-7
N-[3-(4-aminophenyl)propyl]-N,N-dimethylamine

: 1613708-27-2
C₄₁H₅₂N₄O₅

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 529-35-1
5,6,7,8-Tetrahydronaphthalen-1-ol

: 1613708-27-2
C₄₁H₅₂N₄O₅

Guidance literature:: Multi-step reaction with 16 steps

1.1: sodium hydroxide / 2 h / 0 - 20 °C

2.1: trichlorophosphate / dichloromethane / 6 h / 0 - 80 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C

3.2: 16 h / 20 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 760.05 Torr

5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

6.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1.5 h / -78 - -20 °C

6.2: 1.67 h / -78 - 20 °C

7.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

7.2: 0.08 h

7.3: 16 h / 24 °C

8.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.17 h / 0 - 20 °C

9.1: palladium 10% on activated carbon; hydrogen; acetic acid / water / 3 h / 20 °C / 760.05 Torr

10.1: acetic acid; hydrogen bromide / 3 h / Reflux

11.1: acetyl chloride / 4 h / 0 °C / Reflux

12.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

13.1: pyridine / dichloromethane / 3 h / 0 - 20 °C

14.1: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

15.1: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

16.1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetonitrile;

Reference yield:

: 1008-19-1
5-methoxy-1,2,3,4-tetrahydro-naphthalene

: 1613708-27-2
C₄₁H₅₂N₄O₅

Guidance literature:: Multi-step reaction with 15 steps

1.1: trichlorophosphate / dichloromethane / 6 h / 0 - 80 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C

2.2: 16 h / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 760.05 Torr

4.1: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

5.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1.5 h / -78 - -20 °C

5.2: 1.67 h / -78 - 20 °C

6.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

6.2: 0.08 h

6.3: 16 h / 24 °C

7.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.17 h / 0 - 20 °C

8.1: palladium 10% on activated carbon; hydrogen; acetic acid / water / 3 h / 20 °C / 760.05 Torr

9.1: acetic acid; hydrogen bromide / 3 h / Reflux

10.1: acetyl chloride / 4 h / 0 °C / Reflux

11.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

12.1: pyridine / dichloromethane / 3 h / 0 - 20 °C

13.1: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

14.1: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

15.1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetonitrile;