C₃₃H₃₈N₄O₅Si

Base Information

Chemical Name:C₃₃H₃₈N₄O₅Si
CAS No.:1295471-18-9
Molecular Formula:C₃₃H₃₈N₄O₅Si
Molecular Weight:598.774
Hs Code.:

C<sub>33</sub>H<sub>38</sub>N<sub>4</sub>O<sub>5</sub>Si

Synonyms:C₃₃H₃₈N₄O₅Si

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Chemical Property of C₃₃H₃₈N₄O₅Si

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Technology Process of C₃₃H₃₈N₄O₅Si

There total 15 articles about C₃₃H₃₈N₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1295471-17-8
C₃₂H₃₄N₄O₅Si

: 75-16-1
methylmagnesium bromide

: 1295471-18-9
C₃₃H₃₈N₄O₅Si

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-03-2
C₃₉H₅₃NO₅Si₂

: 1295471-18-9
C₃₃H₃₈N₄O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: ozone / dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

3.1: pyridine; trifluoroacetyl chloride / dichloromethane / 8 h / 20 °C

4.1: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane; water / 0 °C

5.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 1.17 h / 0 °C

6.1: pyridine / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

7.1: tetrabutylammoniun azide / toluene / 72 h / 20 °C / Molecular sieve; Inert atmosphere

8.1: water; trifluoroacetic acid / acetonitrile / 4 h / 0 °C / Inert atmosphere

9.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

10.1: tetrahydrofuran; diethyl ether / 3 h / -78 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; chloro-trimethyl-silane; cerium(III) chloride heptahydrate; water; dihydrogen peroxide; tetrabutylammoniun azide; titanium tetrachloride; Dess-Martin periodane; ozone; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetyl chloride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile; 5.1: Luche reduction;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-52-1
C₃₉H₅₅NO₅Si₂

: 1295471-18-9
C₃₃H₃₈N₄O₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 0 °C

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

4.1: pyridine; trifluoroacetyl chloride / dichloromethane / 8 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane; water / 0 °C

6.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 1.17 h / 0 °C

7.1: pyridine / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

8.1: tetrabutylammoniun azide / toluene / 72 h / 20 °C / Molecular sieve; Inert atmosphere

9.1: water; trifluoroacetic acid / acetonitrile / 4 h / 0 °C / Inert atmosphere

10.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

11.1: tetrahydrofuran; diethyl ether / 3 h / -78 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; chloro-trimethyl-silane; oxalyl dichloride; cerium(III) chloride heptahydrate; water; dihydrogen peroxide; tetrabutylammoniun azide; titanium tetrachloride; Dess-Martin periodane; ozone; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetyl chloride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile; 6.1: Luche reduction;
DOI:10.1002/anie.201008079