Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

Base Information

Chemical Name:Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid
CAS No.:202271-47-4
Molecular Formula:C₂₄H₃₅ClO₇
Molecular Weight:470.991
Hs Code.:

Synonyms:Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

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Chemical Property of Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

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Technology Process of Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

There total 2 articles about Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 58341-69-8
methyl 2,3-di-O-allyl-6-O-benzyl-α-D-glucopyranoside

: 111-44-4
3-oxa-1,5-dichloropentane

: 202271-47-4
Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1055/s-1998-4480

Reference yield:

: 13035-23-9,359437-00-6
methyl 4,6-O-benzylidene-2,3-di-O-allyl-α-D-glucopyranoside

: 202271-47-4
Methyl-2,3-di-O-allyl-6-O-benzyl-4-O-[2-(2-chloroethoxy)ethyl]-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaBH₃CN, methyl orange, HCl / tetrahydrofuran; diethyl ether / 1.5 h / Ambient temperature

2: 84 percent / 50percent aq. KOH, TBAHS / tetrahydrofuran / 12 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; methyl orange; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether;
DOI:10.1055/s-1998-4480