3-Bromo-1-methyl-pyridinium iodide

Base Information

• Chemical Name: 3-Bromo-1-methyl-pyridinium iodide
• CAS No.: 32222-42-7
• Molecular Formula: C6H7 Br N . I
• Molecular Weight: 299.937
• DSSTox Substance ID: DTXSID80507123
• Mol file: 32222-42-7.mol

Synonyms:32222-42-7;3-Bromo-1-methyl-pyridinium iodide;3-bromo-1-methylpyridin-1-ium iodide;3-Bromo-1-methylpyridinium iodide;3-bromo-1-methylpyridin-1-ium;iodide;DTXSID80507123;N-Methyl-3-Bromopyridinium iodide;3-bromo-1-methylpyridin-1-iumiodide;MFCD00464927;AKOS015969294;CS-W001537;s12022;J-018680

Chemical Property of 3-Bromo-1-methyl-pyridinium iodide

Chemical Property:

• PSA: 3.88000
• LogP: -1.72240
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 298.88066
• Heavy Atom Count: 9
• Complexity: 74.9

Purity/Quality:

99% ^*data from raw suppliers

3-Bromo-1-methylpyridin-1-iumiodide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=CC=CC(=C1)Br.[I-]

Technology Process of 3-Bromo-1-methyl-pyridinium iodide

There total 2 articles about 3-Bromo-1-methyl-pyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-Bromopyridine (626-55-1,163928-56-1) + methyl iodide (74-88-4) → 3-bromo-N-methylpyridinium iodide (32222-42-7)

Guidance literature:

With ethanol; at 92 ℃; for 16h; Inert atmosphere; Reflux;

DOI:10.1021/cg200942u

Reference yield:

→ 3-bromo-N-methylpyridinium iodide (32222-42-7)

Guidance literature:

3-Brompyridin, MeI;

Reference yield: 80.0%

tributylstannylethynylbenzene (3757-88-8) + 3-bromo-N-methylpyridinium iodide (32222-42-7) → 1-methyl-3-phenylethynyl-pyridinium; iodide

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide;

DOI:10.1055/s-2002-34903

upstream raw materials:

3-Bromopyridine

methyl iodide

Downstream raw materials:

3-Bromopyridine

3-bromo-1-methyl-1,2,5,6-tetrahydropyridine

iodure de 1-methyl-3-phenylpyridinium

1-methyl-3-(m-bromophenylethynyl)pyridinium iodide