N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

Base Information

Chemical Name:N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide
CAS No.:1083078-01-6
Molecular Formula:C₂₅H₃₄N₄O₃SSi₂
Molecular Weight:526.807
Hs Code.:

Synonyms:N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

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Chemical Property of N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

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Technology Process of N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

There total 5 articles about N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₂₇H₃₆N₄O₄SSi₂

: 1083078-01-6
N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

Guidance literature:: With potassium hydroxide; In water; acetonitrile;
DOI:10.1039/c2ob25103e

Reference yield:

: C₂₇H₃₈N₂O₄SSi₂

: 1083078-01-6
N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide / acetonitrile / 2 h / 0 - 20 °C / Inert atmosphere

2: potassium hydroxide / water; acetonitrile

With 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide; potassium hydroxide; In water; acetonitrile;
DOI:10.1039/c2ob25103e

Reference yield:

: 1-phenylsulfonyl-2,3-dimethylindole

: 1083078-01-6
N-[bis(trimethylsilyl)methyl]-N-[(1-phenylsulfonyl-3-methyl-indol-2-yl)methyl]-α-diazoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / tetrahydrofuran / 1.67 h / 0 - 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide / acetonitrile / 2 h / 0 - 20 °C / Inert atmosphere

3: potassium hydroxide / water; acetonitrile

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide; potassium hydroxide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c2ob25103e