1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)-

Base Information

Chemical Name:1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)-
CAS No.:164261-56-7
Molecular Formula:C16H14BrNO2S
Molecular Weight:364.263
Hs Code.:
DSSTox Substance ID:DTXSID50437327
Nikkaji Number:J1.942.397B
Wikidata:Q82252811
Mol file:164261-56-7.mol

Synonyms:1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)-;164261-56-7;DTXSID50437327;1-(Phenylsulfonyl)-2-(bromomethyl)-3-methyl-1H-indole

Suppliers and Price of 1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)-

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:362.99286
Heavy Atom Count:21
Complexity:455

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(N(C2=CC=CC=C12)S(=O)(=O)C3=CC=CC=C3)CBr

Technology Process of 1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)-

There total 4 articles about 1H-Indole, 2-(bromomethyl)-3-methyl-1-(phenylsulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 116325-48-5
N-benzenesulfonyl-2,3-dimethyl-1H-indole

: 164261-56-7
1-(Phenylsulfonyl)-3-methyl-2-(bromomethyl)indole

Guidance literature:: With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; Heating;
DOI:10.1021/jo00112a011

Reference yield:

: 91-55-4
2,3-dimethylindole

: 164261-56-7
1-(Phenylsulfonyl)-3-methyl-2-(bromomethyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 2 h, 2.) THF, from 0 deg C to 5 deg C, 1 h

2: 92 percent / benzoyl peroxide, NBS / CCl₄ / 2 h / Heating

With N-Bromosuccinimide; sodium hydride; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1080/00397919508015445

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 164261-56-7
1-(Phenylsulfonyl)-3-methyl-2-(bromomethyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 2 h, 2.) THF, from 0 deg C to 5 deg C, 1 h

2: 92 percent / benzoyl peroxide, NBS / CCl₄ / 2 h / Heating

With N-Bromosuccinimide; sodium hydride; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1080/00397919508015445