4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

Base Information

Chemical Name:4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride
CAS No.:1321626-13-4
Molecular Formula:C₁₉H₁₁Cl₂NO₄S
Molecular Weight:420.273
Hs Code.:

Synonyms:4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

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Chemical Property of 4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

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Technology Process of 4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

There total 3 articles about 4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 4022-35-9
2-benzyl-6-chloro-1H-benzo[de]isoquinoline-1,3(2H)-dione

: 1321626-13-4
4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

Guidance literature:: With chlorosulfonic acid; at 50 ℃; Cooling;
DOI:10.1016/j.bmc.2011.05.056

Reference yield:

: 100-46-9
benzylamine

: 1321626-13-4
4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / Reflux

2: chlorosulfonic acid / 50 °C / Cooling

With chlorosulfonic acid; In ethanol;
DOI:10.1016/j.bmc.2011.05.056

Reference yield:

: 4053-08-1
p-chloro-1,8-naphthalicanhydride

: 1321626-13-4
4-[(6-chloro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / Reflux

2: chlorosulfonic acid / 50 °C / Cooling

With chlorosulfonic acid; In ethanol;
DOI:10.1016/j.bmc.2011.05.056