C₂₂H₂₄FN₃O₅S

Base Information

Chemical Name:C₂₂H₂₄FN₃O₅S
CAS No.:1374233-64-3
Molecular Formula:C₂₂H₂₄FN₃O₅S
Molecular Weight:461.514
Hs Code.:

C<sub>22</sub>H<sub>24</sub>FN<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₂H₂₄FN₃O₅S

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Chemical Property of C₂₂H₂₄FN₃O₅S

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Technology Process of C₂₂H₂₄FN₃O₅S

There total 6 articles about C₂₂H₂₄FN₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1374233-63-2
C₂₃H₂₆FN₃O₅S

: 1374233-64-3
C₂₂H₂₄FN₃O₅S

Guidance literature:: C₂₃H₂₆FN₃O₅S; With 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate; In N,N-dimethyl-formamide; for 0.5h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; N,N-dimethyl-formamide; at 0 ℃; pH=3 - 4;

Reference yield:

: 31872-62-5
4-methoxy-3-nitro-pyridine

: 1374233-64-3
C₂₂H₂₄FN₃O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 24 h / 20 °C

2.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

3.1: dichloromethane / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

6.1: 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Reflux

6.2: 0 °C / pH 3 - 4

With 2-(diethylamino)ethanethiol hydrochloride; hydrogen; potassium carbonate; triethylamine; sodium t-butanolate; palladium 10% on activated carbon; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 33631-09-3
4-methoxypyridin-3-amine

: 1374233-64-3
C₂₂H₂₄FN₃O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2.1: dichloromethane / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

5.1: 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Reflux

5.2: 0 °C / pH 3 - 4

With 2-(diethylamino)ethanethiol hydrochloride; potassium carbonate; triethylamine; sodium t-butanolate; In dichloromethane; N,N-dimethyl-formamide;