(1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-one

Base Information

• Chemical Name: (1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-one
• CAS No.: 370568-21-1
• Molecular Formula: C₃₀H₃₈OS₂
• Molecular Weight: 478.763

Synonyms:(1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-one

Chemical Property of (1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-one

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Technology Process of (1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-one

There total 2 articles about (1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.0^2,6]deca-4,8-dien-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

carbon monoxide (201230-82-2) + bicyclo[2.2.1]hepta-2,5-diene (121-46-0) + (1R,2R)-2-ethynylsulfanyl-7,7-dimethyl-1-[(2,4,6-trimethylbenzylsulfanyl)methyl]bicyclo[2.2.1]heptane (370568-18-6) → (1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.02,6]deca-4,8-dien-3-one (370568-21-1)

Guidance literature:

carbon monoxide; (1R,2R)-2-ethynylsulfanyl-7,7-dimethyl-1-[(2,4,6-trimethylbenzylsulfanyl)methyl]bicyclo[2.2.1]heptane; With dicobalt octacarbonyl; In hexane; at 20 ℃; for 0.333333h;

In hexane; at 55 ℃;

bicyclo[2.2.1]hepta-2,5-diene; In hexane; at 0 ℃; for 24h; Further stages.;

DOI:10.1021/jo015790p

Reference yield:

carbon monoxide (201230-82-2) + bicyclo[2.2.1]hepta-2,5-diene (121-46-0) + (1R,2R)-2-ethynylsulfanyl-7,7-dimethyl-1-[(2,4,6-trimethylbenzylsulfanyl)methyl]bicyclo[2.2.1]heptane (370568-18-6) → (3aR,4R,7S,7aS)-2-[(1R,2R,4R)-7,7-Dimethyl-1-(2,4,6-trimethyl-benzylsulfanylmethyl)-bicyclo[2.2.1]hept-2-ylsulfanyl]-3a,4,7,7a-tetrahydro-4,7-methano-inden-1-one + (1R,2R,6S,7S)-4-[(1R,2R,4R)-7,7-dimethyl-1-(2,4,6-trimethylbenzylsulfanyl)methylbicyclo[2.2.1]hept-2-ylsulfanyl]tricyclo[5.2.1.02,6]deca-4,8-dien-3-one (370568-21-1)

Guidance literature:

With N-methyl-2-indolinone; dicobalt octacarbonyl; at 0 ℃; for 48h; Title compound not separated from byproducts.;

DOI:10.1021/jo015790p

upstream raw materials:

carbon monoxide

bicyclo[2.2.1]hepta-2,5-diene

(1R,2R)-2-ethynylsulfanyl-7,7-dimethyl-1-[(2,4,6-trimethylbenzylsulfanyl)methyl]bicyclo[2.2.1]heptane

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