O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

Base Information

Chemical Name:O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol
CAS No.:1334671-99-6
Molecular Formula:C₇₆H₈₉Cl₃N₄O₁₆
Molecular Weight:1420.92
Hs Code.:

O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

Synonyms:O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

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Chemical Property of O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

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Technology Process of O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

There total 1 articles about O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1334671-98-5
O-(4,6-di-O-benzyl-2-deoxy-3-O-p-methoxybenzyl-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

: 1334671-99-6
O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.carres.2011.06.027

Reference yield: 67.0%

: 1334671-96-3
phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

: 1334671-99-6
O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

: 1334672-00-2
O-(4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-α-L-fucopyranosyl)-(1->3)-O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol

Guidance literature:: phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside; O-(4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->1)-(2S,3R)-2-azido-3-O-benzoyl-1,3-eicosanediol; With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 0.25h; Molecular sieve;

With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 1h; Molecular sieve;
DOI:10.1016/j.carres.2011.06.027