3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Base Information

Chemical Name:3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide
CAS No.:947530-60-1
Molecular Formula:C₂₁H₂₂BrNO₄
Molecular Weight:432.314
Hs Code.:

Synonyms:3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Suppliers and Price of 3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

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Technology Process of 3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

There total 2 articles about 3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₁₄H₁₁O₅N

: 162330-95-2
β-(2-bromo-4,5-dimethoxyphenyl)-N-methylethylamine

: 947530-60-1
3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Guidance literature:: In 1,4-dioxane; at 20 ℃;
DOI:10.1021/ol071079g

Reference yield:

: 2227-57-8
3-(4-methoxyphenyl)propynoic acid

: 947530-60-1
3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / dioxane / 20 °C

2: 100 percent / dioxane / 20 °C

With dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/ol071079g

Reference yield: 71.0%

: 947530-60-1
3-(4-methoxyphenyl)propynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-methylamide

: 7,8-dimethoxy-1-(4-methoxybenzylidene)-3-methyl-1,3,4,5-tetrahydrobenzo[d]azepin-2-one

Guidance literature:: With sodium formate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 110 ℃; for 0.25h; microwave irradiation;
DOI:10.1021/ol071079g