C₃₉H₄₂N₂O₅SSi

Base Information

Chemical Name:C₃₉H₄₂N₂O₅SSi
CAS No.:1352230-37-5
Molecular Formula:C₃₉H₄₂N₂O₅SSi
Molecular Weight:678.924
Hs Code.:

C<sub>39</sub>H<sub>42</sub>N<sub>2</sub>O<sub>5</sub>SSi

Synonyms:C₃₉H₄₂N₂O₅SSi

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Chemical Property of C₃₉H₄₂N₂O₅SSi

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Technology Process of C₃₉H₄₂N₂O₅SSi

There total 19 articles about C₃₉H₄₂N₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352230-33-1
C₄₁H₄₅F₃N₂O₁₁S₂Si

: 1352230-37-5
C₃₉H₄₂N₂O₅SSi

Guidance literature:: C₄₁H₄₅F₃N₂O₁₁S₂Si; With potassium thioacetate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

With potassium carbonate; In methanol; N,N-dimethyl-formamide; for 12h;

Reference yield:

: 956485-08-8
((3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1352230-37-5
C₃₉H₄₂N₂O₅SSi

Guidance literature:: Multi-step reaction with 10 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

1.2: 1 h / -78 - 20 °C

2.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

2.2: 3 h / -78 °C

2.3: 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: lithium borohydride; methanol / tetrahydrofuran / 2 h / -78 °C

5.1: sulfuric acid / 2 h / 20 °C

6.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

6.2: 0 - 60 °C

7.1: potassium carbonate; methanol

8.1: pyridine

9.1: pyridine / 5.5 h / 0 - 20 °C

10.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

10.2: 12 h

With pyridine; methanol; lithium borohydride; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

(3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde: (3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde

: 1352230-37-5
C₃₉H₄₂N₂O₅SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

1.2: 3 h / -78 °C

1.3: 20 °C

2.1: sulfuric acid / 2 h / 20 °C

3.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

3.2: 0 - 60 °C

4.1: potassium carbonate / methanol / 96 h / 20 °C

4.2: 12 h / 0 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

5.2: 1.5 h

6.1: pyridine / 5.5 h / 0 - 20 °C

7.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

7.2: 12 h

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium thioacetate; sulfuric acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;