Cyclohexanecarboxylic acid, 2-hydroxy-, hydrazide, (1S,2S)- (9CI)

Base Information

• Chemical Name: Cyclohexanecarboxylic acid, 2-hydroxy-, hydrazide, (1S,2S)- (9CI)
• CAS No.: 216879-13-9
• Molecular Formula: C₇H₁₄N₂O₂
• Molecular Weight: 158.2
• Mol file: 216879-13-9.mol

Synonyms:Cyclohexanecarboxylic acid, 2-hydroxy-, hydrazide, (1S,2S)- (9CI)

Chemical Property of Cyclohexanecarboxylic acid, 2-hydroxy-, hydrazide, (1S,2S)- (9CI)

Chemical Property:

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Technology Process of Cyclohexanecarboxylic acid, 2-hydroxy-, hydrazide, (1S,2S)- (9CI)

There total 8 articles about Cyclohexanecarboxylic acid, 2-hydroxy-, hydrazide, (1S,2S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

ethyl (1R,2S)-2-hydroxycyclohexane-1-carboxylate (61586-78-5) → (1R,2S)-2-Hydroxy-cyclohexanecarboxylic acid hydrazide (217311-57-4,216879-13-9,672310-35-9)

Guidance literature:

With hydrazine hydrate; In ethanol; water; for 1h; Heating;

DOI:10.1016/S0957-4166(01)00364-0

Reference yield: 90.0%

cis-ethyl 2-hydroxy-cyclohexanoate (1655-06-7,3444-72-2,6125-55-9,6149-52-6,29569-79-7,61586-78-5,77026-73-4,119068-36-9,119068-37-0) → (+/-)-cis-2-hydroxy-cyclohexane-carboxylic acid-(1)-hydrazide (21651-72-9,21651-73-0,100948-90-1,130023-73-3,130023-74-4,216879-13-9,672310-35-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 1h; Heating;

Reference yield: 87.0%

(+-)-trans-2-hydroxy-cyclohexanecarboxylic acid ethyl ester (1655-06-7,3444-72-2,6125-55-9,6149-52-6,29569-79-7,61586-78-5,77026-73-4,119068-36-9,119068-37-0) → (+/-)-trans-2-hydroxy-cyclohexane-carboxylic acid-(1)-hydrazide (21651-72-9,21651-73-0,100948-90-1,130023-73-3,130023-74-4,216879-13-9,672310-35-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 1h; Heating;

upstream raw materials:

(+/-)-cis-2-hydroxy-cyclohexanecarboxylic acid methyl ester

cis-ethyl 2-hydroxy-cyclohexanoate

trans-2-carbomethoxycyclohexan-1-ol

(+-)-trans-2-hydroxy-cyclohexanecarboxylic acid ethyl ester

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