2,4(1H,3H)-Pyrimidinedione, dihydro-3-methyl-1-(2-methylpropyl)-6-thioxo-

Base Information

Chemical Name:2,4(1H,3H)-Pyrimidinedione, dihydro-3-methyl-1-(2-methylpropyl)-6-thioxo-
CAS No.:216686-76-9
Molecular Formula:C₉H₁₄N₂O₂S
Molecular Weight:214.288
Hs Code.:
Mol file:216686-76-9.mol

Synonyms:6-Mercapto-3-methyl-1-(2-methylpropyl)pyrimidine-2,4(1H,3H)-dione;6-Mercapto-3-methyl-1-(isobutyl)pyrimidine-2,4(1H,3H)-dione

Suppliers and Price of 2,4(1H,3H)-Pyrimidinedione, dihydro-3-methyl-1-(2-methylpropyl)-6-thioxo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 2,4(1H,3H)-Pyrimidinedione, dihydro-3-methyl-1-(2-methylpropyl)-6-thioxo-

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4(1H,3H)-Pyrimidinedione, dihydro-3-methyl-1-(2-methylpropyl)-6-thioxo-

There total 3 articles about 2,4(1H,3H)-Pyrimidinedione, dihydro-3-methyl-1-(2-methylpropyl)-6-thioxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 214636-53-0
6-chloro-3-methyl-1-(2-methylpropyl)-1H-pyrimidine-2,4(1H,3H)-dione

: 216686-76-9
3-methyl-1-(2-methylpropyl)-6-thioxo-pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With sodium hydrogen sulfide monohydrate; In ethanol; at 20 ℃; for 40h; Inert atmosphere;
DOI:10.1016/j.tet.2018.06.019

Reference yield:

: sodium hydrosulfide monohydrate

: 214636-53-0
6-chloro-3-methyl-1-(2-methylpropyl)-1H-pyrimidine-2,4(1H,3H)-dione

: 216686-76-9
3-methyl-1-(2-methylpropyl)-6-thioxo-pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With hydrogenchloride; In ethanol;

Reference yield:

: 4318-56-3
3-methyl-6-chlorouracil

: 216686-76-9
3-methyl-1-(2-methylpropyl)-6-thioxo-pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 48 h / 60 °C

2: sodium hydrogen sulfide monohydrate / ethanol / 40 h / 20 °C / Inert atmosphere

With sodium hydrogen sulfide monohydrate; potassium carbonate; In ethanol; dimethyl sulfoxide;
DOI:10.1016/j.tet.2018.06.019