2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

Base Information

Chemical Name:2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol
CAS No.:1404216-25-6
Molecular Formula:C₁₆H₁₈N₄O₂
Molecular Weight:298.345
Hs Code.:

Synonyms:2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

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Chemical Property of 2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

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Technology Process of 2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

There total 1 articles about 2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1166948-81-7
4-benzyloxy-5H-pyrrolo[3,2-d]pyrimidine-7-carbaldehyde

: 141-43-5
ethanolamine

: 1404216-25-6
2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

Guidance literature:: 4-benzyloxy-5H-pyrrolo[3,2-d]pyrimidine-7-carbaldehyde; ethanolamine; With acetyl chloride; In methanol; at 40 ℃; for 0.5h; pH=5;

With 2-picoline borane complex; In methanol; at 40 ℃; for 4h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1404216-25-6
2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

: 1404216-26-7
tert-butyl N-{[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}-N-(2-hydroxyethyl)carbamate

Guidance literature:: With triethylamine; In methanol; for 0.5h;

Reference yield:

: 1404216-25-6
2-({[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}amino)ethan-1-ol

: 1404216-27-8
tert-butyl N-{[4-(benzyloxy)-5H-pyrrolo[3,2-d]pyrimidin-7-yl]methyl}-N-(2-{[bis(benzyloxy)phosphoryl]oxy}ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 0.5 h

2: 1H-tetrazole / dichloromethane / 0.5 h / Inert atmosphere

With 1H-tetrazole; triethylamine; In methanol; dichloromethane;