3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

Base Information

Chemical Name:3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester
CAS No.:214635-39-9
Molecular Formula:C₂₉H₃₄N₂O₅S₂
Molecular Weight:554.731
Hs Code.:

Synonyms:3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

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Chemical Property of 3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

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Technology Process of 3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

There total 5 articles about 3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39098-91-4
2,2-bis(ethylthio)acetyl chloride

: 2-{3-[(Z)-Benzylimino]-2-methoxycarbonyl-butyl}-indole-1-carboxylic acid methyl ester

: 214635-39-9
3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jo020083x

Reference yield:

: methyl 2-bromomethyl-1-indolecarboxylate

: 214635-39-9
3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / NaH / tetrahydrofuran / 3 h / 20 °C

2: toluene / 8 h / Heating

3: 7.3 g / pyridine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; sodium hydride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo020083x

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 214635-39-9
3-(2,2-diethylthio-N-benzylacetylamino)-2-((1-(methoxycarbonyl)indol-2-yl)methyl)-but-3-enioc acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / NaH / tetrahydrofuran / 3 h / 20 °C

2: toluene / 8 h / Heating

3: 7.3 g / pyridine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; sodium hydride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo020083x