4-(1-phenylacetyl)-1H-cyclobutanaphthalene

Base Information

Chemical Name:4-(1-phenylacetyl)-1H-cyclobutanaphthalene
CAS No.:99018-24-3
Molecular Formula:C₁₉H₁₄O
Molecular Weight:258.32
Hs Code.:

4-(1-phenylacetyl)-1H-cyclobuta<de>naphthalene

Synonyms:4-(1-phenylacetyl)-1H-cyclobutanaphthalene

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Chemical Property of 4-(1-phenylacetyl)-1H-cyclobutanaphthalene

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Technology Process of 4-(1-phenylacetyl)-1H-cyclobutanaphthalene

There total 4 articles about 4-(1-phenylacetyl)-1H-cyclobutanaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 24973-91-9
1H-Cyclobutanaphthalene

: 103-80-0
phenylacetyl chloride

: 99018-24-3
4-(1-phenylacetyl)-1H-cyclobutanaphthalene

Guidance literature:: With aluminium trichloride; In dichloromethane; at 25 ℃; for 8h;
DOI:10.1021/jo00350a053

Reference yield:

: 97383-32-9
2,4-dibromo-1H-cyclobutanaphthalene

: 99018-24-3
4-(1-phenylacetyl)-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium bis(2-methoxyethoxy)aluminum hydride / diethyl ether; benzene / 30 h / Heating

2: 87 percent / AlCl₃ / CH₂Cl₂ / 8 h / 25 °C

With aluminium trichloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00350a053

Reference yield:

: 97383-31-8
1aα,2,3,4α-tetrabromo-1a,2,3,4,-tetrahydro-1H-cyclobutanaphthalene

: 99018-24-3
4-(1-phenylacetyl)-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium bis(2-methoxyethoxy)aluminum hydride / diethyl ether; benzene

2: 87 percent / AlCl₃ / CH₂Cl₂ / 8 h / 25 °C

With aluminium trichloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00350a053