2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

Base Information

Chemical Name:2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol
CAS No.:163563-70-0
Molecular Formula:C₆₄H₆₇O₁₇P₃
Molecular Weight:1201.15
Hs Code.:

Synonyms:2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

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Chemical Property of 2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

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Technology Process of 2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

There total 2 articles about 2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1-O-(4-Methoxybenzyl)-2,6-bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

: 163563-70-0
2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jo00116a023

Reference yield: 84.0%

: 1188371-71-2
2,6-O-bis(benzyloxymethyl)-1-O-(tert-butyldiphenylsilyl)-D-myo-insitol 3,4,5-tris(dibenzyl phosphate)

: 163563-70-0
2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

Guidance literature:: With tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1002/ejoc.200900476

Reference yield: 99.0%

: benzyl N-Cbz-6-aminohexyl diisopropylphosphoramidite

: 163563-70-0
2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

: 1188371-77-8
benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

Guidance literature:: benzyl N-Cbz-6-aminohexyl diisopropylphosphoramidite; 2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 18h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; at -60 - 20 ℃;
DOI:10.1002/ejoc.200900476