benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

Base Information

Chemical Name:benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate
CAS No.:1581734-81-7
Molecular Formula:C₁₃H₁₂F₆O₅S
Molecular Weight:394.292
Hs Code.:

Synonyms:benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

Chemical Property:

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Technology Process of benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

There total 3 articles about benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1581734-80-6
benzyl (2R)-5,5,5-trifluoro-2-hydroxypentanoate

: 1581734-81-7
benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

Guidance literature:: trifluoromethylsulfonic anhydride; With 2,6-dimethylpyridine; In dichloromethane; at -25 ℃; for 0.2h;

benzyl (2R)-5,5,5-trifluoro-2-hydroxypentanoate; In dichloromethane; at -25 ℃; for 0.583333h;

Reference yield:

: 1581734-79-3
(2R)-5,5,5-trifluoro-2-hydroxypentanoic acid

: 1581734-81-7
benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / benzene / 10 h / 50 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 0.2 h / -25 °C

2.2: 0.58 h / -25 °C

With 2,6-dimethylpyridine; sulfuric acid; In dichloromethane; benzene;

Reference yield:

: 122565-29-1,23809-57-6
(2R)-2-amino-5,5,5-trifluoropentanoic acid

: 1581734-81-7
benzyl (2R)-5,5,5-trifluoro-2-{[(trifluoromethyl)sulfonyl]oxy}pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; sodium nitrite / water / 0 - 20 °C

2.1: sulfuric acid / benzene / 10 h / 50 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0.2 h / -25 °C

3.2: 0.58 h / -25 °C

With 2,6-dimethylpyridine; sulfuric acid; sodium nitrite; In dichloromethane; water; benzene;