9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane

Base Information

Chemical Name:9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane
CAS No.:1059700-78-5
Molecular Formula:C₁₆H₂₂N₂
Molecular Weight:242.364
Hs Code.:

9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.1<SP>2,5</SP>]decane

Synonyms:9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane

Chemical Property:

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Technology Process of 9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane

There total 1 articles about 9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 285119-48-4
9-benzyl-9,10-diazatricyclo[4.2.1.1^2,5]decane

: 74-88-4
methyl iodide

: 1059700-78-5
9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2 - 3h;

Reference yield:

: 1059700-78-5
9-benzyl-10-methyl-9,10-diazatricyclo[4.2.1.12,5]decane

: 8-cyclohexyl-N-(N,N-dimethylsulfamoyl)-1,1a,2,12b-tetrahydro-11-methoxy-1a-(9-methyl-9,10-diazatricyclo[4.2.1.12,5]decane-10-carbonyl)cycloprop[d]indolo[2,1-a][2]benzazepine-5-carboxamide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 20 °C

With hydrogenchloride; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; palladium 10% on activated carbon; In ethanol; dichloromethane; water;