7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Base Information

Chemical Name:7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
CAS No.:86619-21-8
Molecular Formula:C₄₀H₅₂N₂O₁₂P₂
Molecular Weight:814.807
Hs Code.:

Synonyms:7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Chemical Property of 7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Technology Process of 7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

There total 5 articles about 7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 69930-74-1
1,10-bis-(2-hydroxyethyl)-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 86619-21-8
7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1) 50 deg C, 2.5 h; 2) r.t., 3 d;

Reference yield:

: 929-59-9,892154-56-2
3,6-dioxa-1,8-diaminooctane

: 86619-21-8
7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 168 h / Heating

2: 49 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 84 percent / methanol / 6 h / 100 °C / 2250.2 Torr

4: 93 percent / 1) NaH / tetrahydrofuran / 1) 50 deg C, 2.5 h; 2) r.t., 3 d

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; methanol; ethanol;

Reference yield:

: 54665-51-9
3,6-dioxaoctanedioic acid dimethylester

: 86619-21-8
7,16-bis<2-(diphenylphosphato)ethyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 168 h / Heating

2: 49 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 84 percent / methanol / 6 h / 100 °C / 2250.2 Torr

4: 93 percent / 1) NaH / tetrahydrofuran / 1) 50 deg C, 2.5 h; 2) r.t., 3 d

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; methanol; ethanol;