(3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

Base Information

Chemical Name:(3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one
CAS No.:1257662-90-0
Molecular Formula:C₂₅H₃₄O₂Si
Molecular Weight:394.629
Hs Code.:

Synonyms:(3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

Suppliers and Price of (3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

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Technology Process of (3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

There total 1 articles about (3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1257663-12-9
(2S,3S,E)-(+)-3-((tert-butyldiphenylsilyloxy)methyl)-N-methoxy-N,2-dimethylhex-4-enamide

: 75-16-1
methylmagnesium bromide

: 1257662-90-0
(3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

Guidance literature:: In tetrahydrofuran; diethyl ether; at -20 - 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/chem.201001133

Reference yield: 65.0%

: 1257662-90-0
(3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one

: 1257662-87-5
C₃₆H₅₆O₇Si₂

: 1257662-97-7
C₅₉H₈₆O₇Si₃

Guidance literature:: (3S,4S,E)-(+)-4-((tert-butyldiphenylsilyloxy)methyl)-3-methylhept-5-en-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;

C₃₆H₅₆O₇Si₂; In tetrahydrofuran; at -78 - 20 ℃; for 1.95h; Inert atmosphere;
DOI:10.1002/chem.201001133