2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

Base Information

Chemical Name:2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide
CAS No.:1386874-99-2
Molecular Formula:C₁₇H₁₄ClN₅O
Molecular Weight:339.784
Hs Code.:

Synonyms:2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

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Chemical Property of 2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

Chemical Property:

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Technology Process of 2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

There total 4 articles about 2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1386874-38-9
ethyl 2-formylquinoline-4-carboxylate

: 1386874-99-2
2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 2 h / 80 °C

2: hydrazine hydrate / 20 h / 120 °C

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1021/jm300146f

Reference yield:

: 7120-26-5
ethyl 2-methylquinoline-4-carboxylate

: 1386874-99-2
2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: selenium(IV) oxide / 1,4-dioxane / 4 h / Reflux

2: acetic acid / ethanol / 2 h / 80 °C

3: hydrazine hydrate / 20 h / 120 °C

With selenium(IV) oxide; hydrazine hydrate; acetic acid; In 1,4-dioxane; ethanol;
DOI:10.1021/jm300146f

Reference yield:

: 634-38-8
2-methylquinoline-4-carboxylic acid

: 1386874-99-2
2-((2-(3-chlorophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 18 h / Reflux

2: selenium(IV) oxide / 1,4-dioxane / 4 h / Reflux

3: acetic acid / ethanol / 2 h / 80 °C

4: hydrazine hydrate / 20 h / 120 °C

With selenium(IV) oxide; sulfuric acid; hydrazine hydrate; acetic acid; In 1,4-dioxane; ethanol;
DOI:10.1021/jm300146f