tetrabutylammonium diphenylbis((methylthio)methyl)borate

Base Information

Chemical Name:tetrabutylammonium diphenylbis((methylthio)methyl)borate
CAS No.:181575-73-5
Molecular Formula:C₁₆H₂₀BS₂*C₁₆H₃₆N
Molecular Weight:529.746
Hs Code.:

Synonyms:tetrabutylammonium diphenylbis((methylthio)methyl)borate

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Chemical Property of tetrabutylammonium diphenylbis((methylthio)methyl)borate

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Technology Process of tetrabutylammonium diphenylbis((methylthio)methyl)borate

There total 1 articles about tetrabutylammonium diphenylbis((methylthio)methyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 74-93-1
methylthiol

: 5123-17-1
bromodiphenylborane

: 1643-19-2
tetrabutylammomium bromide

: 181575-73-5
tetrabutylammonium diphenylbis((methylthio)methyl)borate

Guidance literature:: With n-butyllithium; tetramethylethylenediamine; In tetrahydrofuran; benzene; to methyl sulfide and TMEDA was added n-BuLi in hexane, stirred for 1 h at room temp., heated to 45°C for 1 h, THF was added, cooled to -78°C, a benzene soln. of Ph2BBr was added, warmed to room temp., stirred for 12 h; H2O was added, the organic volatiles were removed under vac., aq. soln. was filtered, (C4H9)4NBr was added, ppt. was filtered, washed with H2O; elem. anal.;
DOI:10.1021/ic010273a

Reference yield: 80.0%

: hexaaquanickel(II) tetrafluoroborate

: 181575-73-5
tetrabutylammonium diphenylbis((methylthio)methyl)borate

: 181575-71-3
Ni(diphenylbis((methylthio)methyl)borate)2

Guidance literature:: In methanol; to soln. (Ni(H2O)6)(BF4)2 in MeOH was added (Bu4N)Ph2Bt; ppt. was filtered, washed with MeOH and dried in vacuo; elem. anal.;
DOI:10.1021/ic010966r

Reference yield: 60.0%

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 181575-73-5
tetrabutylammonium diphenylbis((methylthio)methyl)borate

: ((C₆H₅)2B(CH₂SCH₃)2Cu)4

Guidance literature:: In not given; 10 min; Ohrenberg, C.; Saleem, M. M.; Riordan, C. G.; Yap, G. P. A.; Rheingold, A. L. Chem. Commun. 1996, 1081-1082; dried under vac. at room temp.; elem. anal.;
DOI:10.1021/ic010273a