Technology Process of C20H18O4S
There total 5 articles about C20H18O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
at 45 ℃;
for 12h;
Sealed tube;
DOI:10.1021/ol302166n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl acetamide / 2 h / 160 °C / Sealed tube
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C
3: hydrogenchloride / methanol / 1 h / 20 °C
4: pyridine / 12 h / 45 °C / Sealed tube
With
pyridine; hydrogenchloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/ol302166n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C
2: hydrogenchloride / methanol / 1 h / 20 °C
3: pyridine / 12 h / 45 °C / Sealed tube
With
pyridine; hydrogenchloride; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane;
DOI:10.1021/ol302166n