(R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

Base Information

Chemical Name:(R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium
CAS No.:952797-33-0
Molecular Formula:C₂₈H₃₃NO₂P
Molecular Weight:446.549
Hs Code.:

Synonyms:(R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

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Chemical Property of (R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

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Technology Process of (R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

There total 2 articles about (R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1187932-69-9
(R)-tert-butyl 3-(iodomethyl)pyrrolidine-1-carboxylate

: 603-35-0
triphenylphosphine

: 952797-33-0
(R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 138108-72-2
tert-butyl (R)-3-hydroxymethylpyrrolidine-1-carboxylate

: 952797-33-0
(R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; 1H-imidazole; iodine / dichloromethane / 20 °C

2: N,N-dimethyl-formamide / 2 h / 20 °C

With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 952797-33-0
(R)-((1-(tert-butoxycarbonyl)pyrrolidin-3-yl)methyl)triphenylphosphonium

: methyl 2-((R)-3-(6-oxoheptyl)pyrrolidin-1-yl)-2-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 4 h / 20 °C

2.1: hydrogen; palladium 10% on activated carbon / ethyl acetate / 40 °C

2.2: 2 h / 20 °C

3.1: potassium carbonate / acetonitrile / 40 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; lithium hexamethyldisilazane; In dichloromethane; ethyl acetate; acetonitrile;