3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

Base Information

Chemical Name:3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one
CAS No.:147912-76-3
Molecular Formula:C₃₁H₂₆BrNO₄
Molecular Weight:556.456
Hs Code.:

Synonyms:3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

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Chemical Property of 3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

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Technology Process of 3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

There total 4 articles about 3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 147912-71-8
2--3-(2-bromo-4,5-dimethoxyphenyl)propanoate

: 147912-76-3
3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; water; for 16h; Ambient temperature;
DOI:10.1021/jo00062a018

Reference yield:

: 53207-00-4
1-bromo-2-(bromomethyl)-4,5-dimethoxybenzene

: 147912-76-3
3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

Guidance literature:: Multi-step reaction with 4 steps

2: 80 percent / Pb(NO₃)2, K₃PO₄ / acetonitrile / Ambient temperature

3: 98 percent / LiOH / dioxane; H₂O / 20 h / 60 °C

4: 97 percent / p-toluenesulfonic acid monohydrate / H₂O; tetrahydrofuran / 16 h / Ambient temperature

With lithium hydroxide; potassium phosphate; lead(II) nitrate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile;
DOI:10.1021/jo00062a018

Reference yield:

: 147912-66-1
methyl 2--3-(2-bromo-4,5-dimethoxyphenyl)propanoate

: 147912-76-3
3-(9-phenylfluoren-9-yl)-4-<(2-bromo-4,5-dimethoxyphenyl)methyl>oxazolidin-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / LiOH / dioxane; H₂O / 20 h / 60 °C

2: 97 percent / p-toluenesulfonic acid monohydrate / H₂O; tetrahydrofuran / 16 h / Ambient temperature

With lithium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo00062a018