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Technology Process of SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

Base Information
  • Chemical Name:SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2
  • CAS No.:1266617-63-3
  • Molecular Formula:C31H31BF2N4O2S
  • Molecular Weight:572.487
  • Hs Code.:
SHC<sub>6</sub>H<sub>4</sub>CON<sub>2</sub>C<sub>4</sub>H<sub>8</sub>COC<sub>6</sub>H<sub>4</sub>C<sub>9</sub>H<sub>2</sub>N<sub>2</sub>(CH<sub>3</sub>)4BF<sub>2</sub>

Synonyms:SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

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Chemical Property of SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2
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Technology Process of SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

There total 3 articles about SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C<sub>4</sub>H<sub>8</sub>N<sub>2</sub>HCOC<sub>6</sub>H<sub>4</sub>S<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CON<sub>2</sub>C<sub>4</sub>H<sub>8</sub>COC<sub>6</sub>H<sub>4</sub>C<sub>9</sub>H<sub>2</sub>N<sub>2</sub>(CH<sub>3</sub>)4BF<sub>2</sub>
1266617-62-2

C4H8N2HCOC6H4S2C6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

SHC<sub>6</sub>H<sub>4</sub>CON<sub>2</sub>C<sub>4</sub>H<sub>8</sub>COC<sub>6</sub>H<sub>4</sub>C<sub>9</sub>H<sub>2</sub>N<sub>2</sub>(CH<sub>3</sub>)4BF<sub>2</sub>
1266617-63-3

SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

Guidance literature:
With sodium tetrahydroborate; In tetrahydrofuran; for 0.166667h;
DOI:10.1039/c0cc03806g

Reference yield:

2,5-dioxopyrrolidin-1-yl 4-(4,4-difluoro-1,3,5,7-tetramethyl-3a,4a-diaza-4-bora-s-indacen-8-yl)benzoate
1266617-61-1

2,5-dioxopyrrolidin-1-yl 4-(4,4-difluoro-1,3,5,7-tetramethyl-3a,4a-diaza-4-bora-s-indacen-8-yl)benzoate

SHC<sub>6</sub>H<sub>4</sub>CON<sub>2</sub>C<sub>4</sub>H<sub>8</sub>COC<sub>6</sub>H<sub>4</sub>C<sub>9</sub>H<sub>2</sub>N<sub>2</sub>(CH<sub>3</sub>)4BF<sub>2</sub>
1266617-63-3

SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

Guidance literature:
Multi-step reaction with 2 steps
1: dichloromethane
2: NaBH4 / tetrahydrofuran
With NaBH4; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0cc03806g

Reference yield:

C<sub>4</sub>H<sub>8</sub>N<sub>2</sub>HCOC<sub>6</sub>H<sub>4</sub>S<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CON<sub>2</sub>HC<sub>4</sub>H<sub>8</sub>
1266571-62-3

C4H8N2HCOC6H4S2C6H4CON2HC4H8

SHC<sub>6</sub>H<sub>4</sub>CON<sub>2</sub>C<sub>4</sub>H<sub>8</sub>COC<sub>6</sub>H<sub>4</sub>C<sub>9</sub>H<sub>2</sub>N<sub>2</sub>(CH<sub>3</sub>)4BF<sub>2</sub>
1266617-63-3

SHC6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

Guidance literature:
Multi-step reaction with 2 steps
1: dichloromethane
2: NaBH4 / tetrahydrofuran
With NaBH4; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0cc03806g
upstream raw materials:

C4H8N2HCOC6H4S2C6H4CON2C4H8COC6H4C9H2N2(CH3)4BF2

C4H8N2HCOC6H4S2C6H4CON2HC4H8

2,5-dioxopyrrolidin-1-yl 4-(4,4-difluoro-1,3,5,7-tetramethyl-3a,4a-diaza-4-bora-s-indacen-8-yl)benzoate

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