(S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Base Information

Chemical Name:(S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide
CAS No.:1393677-08-1
Molecular Formula:C₂₇H₃₁NO₄P*I
Molecular Weight:591.426
Hs Code.:

Synonyms:(S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Suppliers and Price of (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

There total 8 articles about (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1393677-12-7
allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

: 1393677-08-1
(S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diethylamine; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo3013622

Reference yield:

: 1393677-10-5
allyl (S)-4-iodo-2-[N,N-bis(tert-butyloxycarbonyl)amino]butanoate

: 1393677-08-1
(S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Guidance literature:: Multi-step reaction with 3 steps

1: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 20 °C / Inert atmosphere

2: neat (no solvent) / 2 h / 80 °C / Inert atmosphere

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diethylamine; 1,2-bis-(diphenylphosphino)ethane / tetrahydrofuran / 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cerium(III) chloride heptahydrate; diethylamine; 1,2-bis-(diphenylphosphino)ethane; sodium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo3013622

Reference yield:

: 1426140-79-5
allyl (S)-2-[bis(t-butyloxycarbonyl)amino]-4-oxobutanoate

: 1393677-08-1
(S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoic acid iodide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / tetrahydrofuran; water / 0.5 h / 0 °C / Inert atmosphere

2: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 20 °C / Inert atmosphere

4: neat (no solvent) / 2 h / 80 °C / Inert atmosphere

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diethylamine; 1,2-bis-(diphenylphosphino)ethane / tetrahydrofuran / 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cerium(III) chloride heptahydrate; iodine; diethylamine; triphenylphosphine; 1,2-bis-(diphenylphosphino)ethane; sodium iodide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jo3013622