C₂₆H₃₆N₂O₉Si

Base Information

Chemical Name:C₂₆H₃₆N₂O₉Si
CAS No.:1450984-46-9
Molecular Formula:C₂₆H₃₆N₂O₉Si
Molecular Weight:548.665
Hs Code.:

C<sub>26</sub>H<sub>36</sub>N<sub>2</sub>O<sub>9</sub>Si

Synonyms:C₂₆H₃₆N₂O₉Si

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Chemical Property of C₂₆H₃₆N₂O₉Si

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Technology Process of C₂₆H₃₆N₂O₉Si

There total 13 articles about C₂₆H₃₆N₂O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 337975-48-1
benzyl (2S,4S,5R)-4-acetoxy-2-carboxy-5-[(tert-butyldimethylsilyloxy)methyl]pyrrolidine-1-carboxylate

: 1450984-46-9
C₂₆H₃₆N₂O₉Si

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1039/c3md00033h

Reference yield:

: 6081-61-4
N-(benzyloxycarbonyl)-D-serine

: 1450984-46-9
C₂₆H₃₆N₂O₉Si

Guidance literature:: Multi-step reaction with 12 steps

1: 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1.5 h / 0 - 25 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / acetone / 15 h / 25 °C / Inert atmosphere

3: diethyl ether / 2 h / -78 °C / Inert atmosphere

4: zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate / methanol / 2.5 h / 0 - 25 °C / Inert atmosphere

5: water; acetic acid / 15 h / 50 °C

6: pyridine / 1 h / 0 °C / Inert atmosphere

7: pyridine / 0.67 h / 0 - 25 °C / Inert atmosphere

8: acetonitrile / 1.5 h / 0 - 25 °C / Inert atmosphere

9: sodium chloride / ethyl acetate; water; acetonitrile / 0.5 h / 25 °C

10: sodium tetrahydroborate; oxygen / N,N-dimethyl-formamide / 3 h / 25 °C

11: ruthenium(III) chloride trihydrate; sodium periodate / water; acetonitrile; tetrachloromethane / 0 °C

12: dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

With 4-methyl-morpholine; pyridine; sodium tetrahydroborate; sodium periodate; zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate; ruthenium(III) chloride trihydrate; boron trifluoride diethyl etherate; water; oxygen; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; sodium chloride; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c3md00033h

Reference yield:

: 1092473-80-7
(R)-benzyl 3-hydroxy-1-(methoxy(methyl)amino)-1-oxopropane-2-ylcarbamate

: 1450984-46-9
C₂₆H₃₆N₂O₉Si

Guidance literature:: Multi-step reaction with 11 steps

1: boron trifluoride diethyl etherate / acetone / 15 h / 25 °C / Inert atmosphere

2: diethyl ether / 2 h / -78 °C / Inert atmosphere

3: zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate / methanol / 2.5 h / 0 - 25 °C / Inert atmosphere

4: water; acetic acid / 15 h / 50 °C

5: pyridine / 1 h / 0 °C / Inert atmosphere

6: pyridine / 0.67 h / 0 - 25 °C / Inert atmosphere

7: acetonitrile / 1.5 h / 0 - 25 °C / Inert atmosphere

8: sodium chloride / ethyl acetate; water; acetonitrile / 0.5 h / 25 °C

9: sodium tetrahydroborate; oxygen / N,N-dimethyl-formamide / 3 h / 25 °C

10: ruthenium(III) chloride trihydrate; sodium periodate / water; acetonitrile; tetrachloromethane / 0 °C

11: dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; sodium periodate; zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate; ruthenium(III) chloride trihydrate; boron trifluoride diethyl etherate; water; oxygen; acetic acid; dicyclohexyl-carbodiimide; sodium chloride; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; water; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c3md00033h