3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

Base Information

Chemical Name:3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose
CAS No.:252052-95-2
Molecular Formula:C₂₂H₃₁NO₅
Molecular Weight:389.492
Hs Code.:

Synonyms:3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

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Chemical Property of 3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

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Technology Process of 3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

There total 4 articles about 3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-39-0
benzyl bromide

: 252052-92-9
3-deoxy-3-allylamino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 252052-95-2
3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

Guidance literature:: With potassium carbonate; In acetone; at 25 ℃; for 20h;
DOI:10.1016/S0040-4020(99)00694-8

Reference yield:

: 2847-00-9
1,2:5,6-di-O-isopropylidene-α-D-hexofuran-3-ulose

: 252052-95-2
3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 3A molecular sieves / benzene / 8 h / Heating

2: NaBH₄ / methanol / 8 h / 0 °C

3: 86 percent / K₂CO₃ / acetone / 20 h / 25 °C

With sodium tetrahydroborate; 3 A molecular sieve; potassium carbonate; In methanol; acetone; benzene; 1: Condensation / 2: Reduction / 3: Alkylation;
DOI:10.1016/S0040-4020(99)00694-8

Reference yield:

: 876593-73-6
Allyl-[(3aR,5S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-dihydro-furo[2,3-d][1,3]dioxol-(6E)-ylidene]-amine

: 252052-95-2
3-deoxy-3-allyl(benzyl)amino-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 8 h / 0 °C

2: 86 percent / K₂CO₃ / acetone / 20 h / 25 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; acetone; 1: Reduction / 2: Alkylation;
DOI:10.1016/S0040-4020(99)00694-8