C₃₀H₃₀FN₅O₄S

Base Information

Chemical Name:C₃₀H₃₀FN₅O₄S
CAS No.:868287-86-9
Molecular Formula:C₃₀H₃₀FN₅O₄S
Molecular Weight:575.664
Hs Code.:

C<sub>30</sub>H<sub>30</sub>FN<sub>5</sub>O<sub>4</sub>S

Synonyms:C₃₀H₃₀FN₅O₄S

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Chemical Property of C₃₀H₃₀FN₅O₄S

Chemical Property:

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Technology Process of C₃₀H₃₀FN₅O₄S

There total 13 articles about C₃₀H₃₀FN₅O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-[1-(4-fluorophenyl)ethyl]-3-[5-(1-hydroxy-1-methyl-2-phenylethyl)-2-furyl]-5-[methyl(methylsulfonyl)amino]benzamide

: C₃₀H₂₉FN₂O₄S

: 868287-86-9
C₃₀H₃₀FN₅O₄S

Guidance literature:: With sodium azide; trifluoroacetic acid; In chloroform; for 1h;

Reference yield:

: 695216-00-3
3-[(methylsulfonyl)amino]-5-nitrobenzoic acid methyl ester

: 868287-86-9
C₃₀H₃₀FN₅O₄S

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

2.1: methanol; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

2.2: 20 °C / pH < 1

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 65 h / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

5.1: tetrafluoroboric acid / water; acetonitrile / 0.67 h / 0 - 20 °C

5.2: 1 h / 0 °C

6.1: diisopropylamine / palladium diacetate; trisulfonated triphenylphosphine trisodium salt / DMF (N,N-dimethyl-formamide) / 15 h / 20 °C

7.1: tetrahydrofuran / 0 - 20 °C

7.2: 20 °C

8.1: Dess-Martin periodane / dichloromethane / 4 h

9.1: tetrahydrofuran / 2 h / 0 °C

10.1: sodium azide; trifluoroacetic acid / chloroform / 1 h

With methanol; sodium hydroxide; tetrafluoroboric acid; sodium azide; 1-hydroxy-7-aza-benzotriazole; hydrogen; sodium hydride; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diisopropylamine; trifluoroacetic acid; palladium diacetate; trisulfonated triphenylphosphine trisodium salt; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; chloroform; water; acetonitrile; 7.1: Grignard Addition / 9.1: Grignard Addition / 10.1: Ritter Reaction;

Reference yield:

: 695216-01-4
3-[methyl(methylsulfonyl)amino]-5-nitrobenzoic acid methyl ester

: 868287-86-9
C₃₀H₃₀FN₅O₄S

Guidance literature:: Multi-step reaction with 9 steps

1.1: methanol; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

1.2: 20 °C / pH < 1

2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 65 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

4.1: tetrafluoroboric acid / water; acetonitrile / 0.67 h / 0 - 20 °C

4.2: 1 h / 0 °C

5.1: diisopropylamine / palladium diacetate; trisulfonated triphenylphosphine trisodium salt / DMF (N,N-dimethyl-formamide) / 15 h / 20 °C

6.1: tetrahydrofuran / 0 - 20 °C

6.2: 20 °C

7.1: Dess-Martin periodane / dichloromethane / 4 h

8.1: tetrahydrofuran / 2 h / 0 °C

9.1: sodium azide; trifluoroacetic acid / chloroform / 1 h

With methanol; sodium hydroxide; tetrafluoroboric acid; sodium azide; 1-hydroxy-7-aza-benzotriazole; hydrogen; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diisopropylamine; trifluoroacetic acid; palladium diacetate; trisulfonated triphenylphosphine trisodium salt; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; chloroform; water; acetonitrile; 6.1: Grignard Addition / 8.1: Grignard Addition / 9.1: Ritter Reaction;