N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

Base Information

Chemical Name:N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide
CAS No.:134899-61-9
Molecular Formula:C₂₁H₁₈ClN₃O₄S
Molecular Weight:443.911
Hs Code.:

Synonyms:N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

Suppliers and Price of N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

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Technology Process of N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

There total 2 articles about N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 128799-92-8
N-tosyl-p-nitro-aniline sodium salt

: m-Chloroacetophenoxime tosylate

: 134899-61-9
N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

Guidance literature:: In 1,4-dioxane; for 12h; Heating;
DOI:10.1248/cpb.39.558

Reference yield:

: 24280-07-7
1-(3-chlorophenyl)ethanone oxime

: 134899-61-9
N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dioxane / 24 h / ice box

2: 24 percent / dioxane / 12 h / Heating

With triethylamine; In 1,4-dioxane;
DOI:10.1248/cpb.39.558

Reference yield:

: 64-17-5
ethanol

: 134899-61-9
N-{1-[(E)-3-Chloro-phenylimino]-ethyl}-4-methyl-N-(4-nitro-phenyl)-benzenesulfonamide

: 734-25-8
N-(4-nitrophenyl)-4-methylbenzenesulfonamide

: 26431-35-6
Ethyl N-(m-chlorophenyl)acetimidate

Guidance literature:: With sodium ethanolate; In tetrahydrofuran; ethanol; at 25 ℃; Rate constant; Mechanism; variation of NaOEt-concentration;
DOI:10.1248/cpb.39.558