C₂₃H₃₁N₃O₆

Base Information

Chemical Name:C₂₃H₃₁N₃O₆
CAS No.:1288961-33-0
Molecular Formula:C₂₃H₃₁N₃O₆
Molecular Weight:445.516
Hs Code.:

C<sub>23</sub>H<sub>31</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₂₃H₃₁N₃O₆

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Chemical Property of C₂₃H₃₁N₃O₆

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Technology Process of C₂₃H₃₁N₃O₆

There total 10 articles about C₂₃H₃₁N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1288961-31-8
tert-butyl (3-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-N-(1,3-dioxan-5-ylmethyl)-6-ethyl-2-methylpyrazolo[5,1-b][1,3]oxazol-7-yl)carbamate

: 1288961-33-0
C₂₃H₃₁N₃O₆

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 10 - 35 ℃; for 1h;

Reference yield:

: 114973-04-5
2,6-dimethoxy-4-methoxymethylbenzaldehyde

: 1288961-33-0
C₂₃H₃₁N₃O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 0.5 h / Cooling with ice

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane; acetonitrile / 15 h / 10 - 35 °C / Molecular sieve

3.1: triethylamine / tetrahydrofuran / 0.33 h / Cooling with ice

3.2: 0.5 h / 0 - 35 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

5.1: toluene-4-sulfonic acid / 4 h / 160 °C / 2250.23 Torr / Microwave irradiation

6.1: hydrogenchloride; sodium nitrite / water / 0.5 h / Cooling with ice

7.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 1 h / 760.05 Torr

8.1: triethylamine / tetrahydrofuran / 4 h / 10 - 35 °C

9.1: sodium hydroxide / dimethyl sulfoxide / 2 h / 10 - 50 °C

10.1: trifluoroacetic acid / dichloromethane / 1 h / 10 - 35 °C

With hydrogenchloride; tetrapropylammonium perruthennate; hydrogen; caesium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; sodium hydroxide; sodium nitrite; 5% Pd(II)/C(eggshell); In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1288961-19-2
1-[2,6-dimethoxy-4-(methoxymethyl)phenyl]propan-1-one

: 1288961-33-0
C₂₃H₃₁N₃O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / tetrahydrofuran / 0.33 h / Cooling with ice

1.2: 0.5 h / 0 - 35 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

3.1: toluene-4-sulfonic acid / 4 h / 160 °C / 2250.23 Torr / Microwave irradiation

4.1: hydrogenchloride; sodium nitrite / water / 0.5 h / Cooling with ice

5.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 1 h / 760.05 Torr

6.1: triethylamine / tetrahydrofuran / 4 h / 10 - 35 °C

7.1: sodium hydroxide / dimethyl sulfoxide / 2 h / 10 - 50 °C

8.1: trifluoroacetic acid / dichloromethane / 1 h / 10 - 35 °C

With hydrogenchloride; hydrogen; caesium carbonate; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; sodium nitrite; 5% Pd(II)/C(eggshell); In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;