1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

Base Information

Chemical Name:1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate
CAS No.:440105-01-1
Molecular Formula:C₄₀H₃₆O₇
Molecular Weight:628.722
Hs Code.:

Synonyms:1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

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Chemical Property of 1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

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Technology Process of 1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

There total 3 articles about 1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 100-39-0
benzyl bromide

: 440105-04-4
2-[2,6-dibenzyloxy-4-(1,1-dimethylethoxycarbonyl)benzoyl]benzoic acid

: 440105-01-1
1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jm020018f

Reference yield:

: 85-44-9
phthalic anhydride

: 440105-01-1
1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -72 °C

1.2: tetrahydrofuran; hexane / 1.5 h / -72 °C

2.1: 59 percent / K₂CO₃ / dimethylformamide / 16 h / 20 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jm020018f

Reference yield:

: 158980-57-5
3,5-dibenzyloxy-4-bromobenzoic acid tert-butyl ester

: 440105-01-1
1,1-dimethylethyl-4-[2-(benzyloxycarbonyl)benzoyl]-3,5-dibenzyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -72 °C

1.2: tetrahydrofuran; hexane / 1.5 h / -72 °C

2.1: 59 percent / K₂CO₃ / dimethylformamide / 16 h / 20 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jm020018f