Technology Process of C53H36N2O2
There total 4 articles about C53H36N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
diethoxyphosphoryl-acetic acid ethyl ester; C51H34N2O;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
Inert atmosphere;
With
hydrogenchloride;
In
tetrahydrofuran; water;
Inert atmosphere;
DOI:10.1007/s10895-010-0697-y
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tetrahydrofuran
2.1: tetrabutylammomium bromide; potassium carbonate / water; toluene / 0.5 h / 20 °C / Inert atmosphere
2.2: 24 h / 90 °C / Inert atmosphere
3.1: potassium tert-butylate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
potassium tert-butylate; tetrabutylammomium bromide; potassium carbonate;
In
tetrahydrofuran; water; toluene;
3.1: Wittig-Horner reaction;
DOI:10.1007/s10895-010-0697-y
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / N,N-dimethyl-formamide
2.1: potassium tert-butylate / tetrahydrofuran
3.1: tetrabutylammomium bromide; potassium carbonate / water; toluene / 0.5 h / 20 °C / Inert atmosphere
3.2: 24 h / 90 °C / Inert atmosphere
4.1: potassium tert-butylate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
4.2: Inert atmosphere
With
potassium tert-butylate; tetrabutylammomium bromide; potassium carbonate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
4.1: Wittig-Horner reaction;
DOI:10.1007/s10895-010-0697-y
