2,4-(2-isopropylphenylimino)-3,3-dimethylpentane

Base Information

• Chemical Name: 2,4-(2-isopropylphenylimino)-3,3-dimethylpentane
• CAS No.: 613686-02-5
• Molecular Formula: C₂₅H₃₄N₂
• Molecular Weight: 362.558
• Mol file: 613686-02-5.mol

Synonyms:2,4-(2-isopropylphenylimino)-3,3-dimethylpentane

Chemical Property of 2,4-(2-isopropylphenylimino)-3,3-dimethylpentane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-(2-isopropylphenylimino)-3,3-dimethylpentane

There total 1 articles about 2,4-(2-isopropylphenylimino)-3,3-dimethylpentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-(2-isopropyl)phenylamino-4-(2-isopropyl)phenyliminopent-2-ene + methyl iodide (74-88-4) → 2,4-(2-isopropylphenylimino)-3,3-dimethylpentane (613686-02-5)

Guidance literature:

2-(2-isopropyl)phenylamino-4-(2-isopropyl)phenyliminopent-2-ene; With n-butyllithium; In hexane; at 22 ℃;

methyl iodide; In hexane; at 0 - 22 ℃; Further stages.;

DOI:10.1039/b212079h

Reference yield:

2,4-(2-isopropylphenylimino)-3,3-dimethylpentane (613686-02-5) → u-1,3-(2-isopropylphenyl)-4,5,5,6-tetramethyl-1,3,2-diazaborinane + 1,3-bis(2-isopropylphenyl)-4,5,5,6-tetramethyl-1,3,2-diazaborinane

Guidance literature:

With tetrabutylammonium borohydride; methyl iodide; In dichloromethane; at 0 ℃; for 6h; Title compound not separated from byproducts.;

DOI:10.1039/b306401h

Reference yield:

2,4-(2-isopropylphenylimino)-3,3-dimethylpentane (613686-02-5) → u-N,N'-bis-(2-isopropylphenyl)-3,3'-dimethylpentane-2,4-diamine

Guidance literature:

Multi-step reaction with 2 steps

1: (Bu)4NBH₄; MeI / CH₂Cl₂ / 6 h / 0 °C

2: aq. HCl / tetrahydrofuran

With hydrogenchloride; tetrabutylammonium borohydride; methyl iodide; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b306401h

upstream raw materials:

methyl iodide