1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI)

Base Information

Chemical Name:1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI)
CAS No.:215032-10-3
Molecular Formula:C₁₀H₂₀O₂
Molecular Weight:172.268
Hs Code.:
Mol file:215032-10-3.mol

Synonyms:1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI)

Suppliers and Price of 1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI)

Chemical Property:

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Technology Process of 1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI)

There total 8 articles about 1,3-Cyclohexanediol,5-methyl-2-(1-methylethyl)-,(1R,2alpha,3R,5bta)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.8%

: 2216-51-5
(-)-menthol

: 91739-72-9
Trans-p-Menthane-3,8-diol

: 200573-67-7
(1R,2S,5R)-2-[2'-hydroxy-10-methylethyl]-5-methylcyclohexan-1-ol

: 18374-79-3
(-)-(1S,3R,4S,6S)-6-hydroxymenthol

: 215032-10-3
3α-hydroxymenthol

Guidance literature:: In acetone; for 288h; Further byproducts given; Cephalosporium aphidicola;
DOI:10.1021/np980057n

Reference yield: 2.3%

: 2216-51-5
(-)-menthol

: 200573-67-7
(1R,2S,5R)-2-[2'-hydroxy-10-methylethyl]-5-methylcyclohexan-1-ol

: 18374-79-3
(-)-(1S,3R,4S,6S)-6-hydroxymenthol

: 140860-15-7,155348-07-5,155348-04-2
(+)-7-hydroxymenthol

: 215032-10-3
3α-hydroxymenthol

Guidance literature:: In acetone; for 288h; Further byproducts given; Cephalosporium aphidicola;
DOI:10.1021/np980057n

Reference yield:

: 1753-40-8
(R)-4-menthen-3-one

: 215032-10-3
(1R,3S)-5-methyl-2-(1-methylethyl)cyclohexane-1,3-diol

: 215032-10-3
(1R,3R)-5-methyl-2-(1-methylethyl)cyclohexane-1,3-diol

Guidance literature:: (R)-4-menthen-3-one; With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; at 20 ℃; for 3.5h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; for 16h; Overall yield = 93 %; Overall yield = 0.73 g; stereospecific reaction; Inert atmosphere;
DOI:10.1007/s10600-013-0443-1