3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

Base Information

Chemical Name:3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose
CAS No.:98870-88-3
Molecular Formula:C₄₁H₅₂O₁₂Si
Molecular Weight:764.942
Hs Code.:

Synonyms:3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

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Technology Process of 3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

There total 1 articles about 3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.9%

: 98-88-4
benzoyl chloride

: 98870-84-9
6'-O-tert-butyldiphenylsilyl-2,1'-4,6-di-O-isopropylidenesucrose

: 98870-88-3
3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

: 98870-87-2
C₄₈H₅₆O₁₃Si

: 98870-90-7
C₄₈H₅₆O₁₃Si

: 98870-89-4
C₅₅H₆₀O₁₄Si

Guidance literature:: In pyridine; for 18h; Ambient temperature;
DOI:10.1016/0008-6215(85)90017-5

Reference yield: 80.0%

: 98870-88-3
3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

: 98870-92-9
3'-O-benzoyl-6'-O-tert-butyldiphenylsilylsucrose

Guidance literature:: With acetic acid; In water; at 50 ℃;
DOI:10.1016/0008-6215(85)90017-5

Reference yield:

: 98870-88-3
3'-O-benzoyl-O-tert-butyldiphenylsilyl-2,1':4,6-di-O-isopropylidenesucrose

: 98870-94-1
6,1',3'-tri-O-benzoyl-6'-O-tert-butyldiphenylsilylsucrose

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 60percent acetic acid / H₂O / 50 °C

2: 15 percent / pyridine / 24 h / Ambient temperature

With acetic acid; In pyridine; water;
DOI:10.1016/0008-6215(85)90017-5