{(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)^(2-)-N,O,O'}dioxouranium-methanol (1/1)

Base Information

• Chemical Name: {(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)^(2-)-N,O,O'}dioxouranium-methanol (1/1)
• CAS No.: 156920-07-9
• Molecular Formula: CH₄O*C₂₂H₁₈N₂O₇U
• Molecular Weight: 692.465

Synonyms:{(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)^(2-)-N,O,O'}dioxouranium-methanol (1/1)

Chemical Property of {(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)^(2-)-N,O,O'}dioxouranium-methanol (1/1)

Chemical Property:

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Technology Process of {(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)^(2-)-N,O,O'}dioxouranium-methanol (1/1)

There total 1 articles about {(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)^(2-)-N,O,O'}dioxouranium-methanol (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

uranyl(VI) acetate dihydrate + 2-amino-phenol (95-55-6) + 2-<2-(3-formyl-2-hydroxyphenoxy)ethoxy>benzenecarboxamide (154824-41-6) → {(2-(1-nitrilomethylidyne)-2-oxyphenylene)-6-(2-(2-(aminocarbonyl)phenoxy)ethoxyphenolato)(2-)-N,O,O'}dioxouranium-methanol (1/1) (156920-07-9)

Guidance literature:

With methanol; In methanol; under Ar; the aldehyde and the amine were refluxed in methanol for 1 h, UO2(OAc)2 in methanol was added, refluxed for 1 h; filtered, washed with methanol; elem. anal.;

DOI:10.1021/ja00089a023

upstream raw materials:

2-amino-phenol

2-<2-(3-formyl-2-hydroxyphenoxy)ethoxy>benzenecarboxamide

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