2,2-dimethyl-4-phenyl-1,3-oxazolidine

Base Information

Chemical Name:2,2-dimethyl-4-phenyl-1,3-oxazolidine
CAS No.:124619-62-1
Molecular Formula:C₁₁H₁₅NO
Molecular Weight:177.246
Hs Code.:

Synonyms:2,2-dimethyl-4-phenyl-1,3-oxazolidine

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Chemical Property of 2,2-dimethyl-4-phenyl-1,3-oxazolidine

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Technology Process of 2,2-dimethyl-4-phenyl-1,3-oxazolidine

There total 1 articles about 2,2-dimethyl-4-phenyl-1,3-oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-64-1
acetone

: 20989-17-7,56613-80-0,71006-16-1,7568-92-5,188586-38-1
Phenylglycinol

: 124619-62-1
2,2-dimethyl-4-phenyl-1,3-oxazolidine

Guidance literature:: With sodium sulfate; In 1,2-dichloro-ethane; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/jo9011255

Reference yield: 94.0%

: 124619-62-1
2,2-dimethyl-4-phenyl-1,3-oxazolidine

: 60180-61-2
methyl diazomalonyl chloride

: 1182263-41-7
2-diazo-3-(2,2-dimethyl-4-phenyl-oxazolidin-3-yl)-3-oxo-propionic acid methyl ester

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo9011255

Reference yield: 31.0%

: 15975-93-6
pentacarbonyl((methyl)((tetramethylammonio)oxy)carbene)chromium⁽⁰⁾

: 124619-62-1
2,2-dimethyl-4-phenyl-1,3-oxazolidine

: 124685-70-7
pentacarbonyl{((5S)-1-aza-2,2-dimethyl-3-oxa-5-phenylcyclopentyl)(methyl)carbene}chromium⁽⁰⁾

Guidance literature:: With 4-methyl-morpholine; Acetyl bromide; In dichloromethane; Cr-complex soln. is deoxygenated, cooled to -40°C under Ar, CH3COBr is added, soln. is stirred for 30 min at -40°C, soln. of oxazolidine and N-methylmorpholine is added, after 30 min warming to -10°C (2 h); neutral alumina is added, filtn. (Celite), filtrate is concd. in vac., adsorbed on silica gel, dried in vac., chromy. (silica gel, hexane, EtOac), recrystn. (EtOac/hexane), elem. anal.; single rotamer by H-NMR; 22% of open chain complex is also obtained;