C₁₆H₂₀⁽²⁾HNO₄

Base Information

• Chemical Name: C₁₆H₂₀⁽²⁾HNO₄
• CAS No.: 119529-54-3
• Molecular Formula: C₁₆H₂₁NO₄
• Molecular Weight: 292.339
• Mol file: 119529-54-3.mol

Synonyms:C₁₆H₂₀⁽²⁾HNO₄

Chemical Property of C₁₆H₂₀⁽²⁾HNO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₂₀⁽²⁾HNO₄

There total 4 articles about C₁₆H₂₀⁽²⁾HNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-2-Methyl-3-phenylamino-but-2-enedioic acid diethyl ester (59916-78-8) → C16H20(2)HNO4 (119529-54-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / t-BuOK / 18-crown-6 / benzene / 24 h / Ambient temperature

2: EtOD / 0.08 h / Ambient temperature; vitamin B_12s

With ethyl [2]alcohol; potassium tert-butylate; 18-crown-6 ether; In benzene;

DOI:10.1021/ja00188a061

Reference yield:

aniline (62-53-3) → C16H20(2)HNO4 (119529-54-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 87 percent / p-toluenesulfonic acid / benzene / 48 h / Heating

2: 77 percent / t-BuOK / 18-crown-6 / benzene / 24 h / Ambient temperature

3: EtOD / 0.08 h / Ambient temperature; vitamin B_12s

With ethyl [2]alcohol; potassium tert-butylate; toluene-4-sulfonic acid; 18-crown-6 ether; In benzene;

DOI:10.1021/ja00188a061

Reference yield:

2-Bromomethyl-2-methyl-3-[(Z)-phenylimino]-succinic acid diethyl ester (119529-51-0) → C16H20(2)HNO4 (119529-54-3)

Guidance literature:

With ethyl [2]alcohol; for 0.0833333h; Ambient temperature; vitamin B_12s;

DOI:10.1021/ja00188a061

upstream raw materials:

2-Bromomethyl-2-methyl-3-[(Z)-phenylimino]-succinic acid diethyl ester

2-Iodomethyl-2-methyl-3-[(Z)-phenylimino]-succinic acid diethyl ester

(Z)-2-Methyl-3-phenylamino-but-2-enedioic acid diethyl ester

aniline