Technology Process of antimycin A3b
There total 8 articles about antimycin A3b which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dibutyl-BOTf; triethylamine
2: lithium hydroxide; dihydrogen peroxide
3: dmap; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / Pd/O
4: dmap; diethylamine
5: tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
6: acetic acid / diethyl ether
With
dmap; lithium hydroxide; dibutyl-BOTf; tetrabutyl ammonium fluoride; hydrogen; dihydrogen peroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; triethylamine;
Pd/O;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / Pd/O
2: dmap; diethylamine
3: tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
4: acetic acid / diethyl ether
With
dmap; tetrabutyl ammonium fluoride; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine;
Pd/O;
In
diethyl ether;
