antimycin A3

Base Information

Chemical Name:antimycin A3
CAS No.:22083-60-9
Molecular Formula:C₂₆H₃₆N₂O₉
Molecular Weight:520.58
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of antimycin A3

Chemical Property:

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Technology Process of antimycin A3

There total 31 articles about antimycin A3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 896434-12-1
3-Methyl-butyric acid (2R,3S,6S,7R,8R)-3-(2-benzyloxy-3-formylamino-benzoylamino)-8-butyl-2,6-dimethyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

: 22083-60-9,41955-14-0,116095-17-1,139066-86-7
antimycin A3

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 30 ℃; for 6.5h; under 760 Torr;
DOI:10.1021/jo0604890

Reference yield:

: 53346-04-6
3-Methyl-butyric acid (2R,3S,6S,7R,8R)-3-amino-8-butyl-2,6-dimethyl-4,9-dioxo-[1,5]dioxonan-7-yl ester

: 22083-60-9,41955-14-0,116095-17-1,139066-86-7
antimycin A3

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / HOBt; EDC*HCl; N-methylmorpholine / dimethylformamide / 23 h / 30 °C

2: 100 percent / hydrogen / Pd/C / ethyl acetate / 6.5 h / 30 °C / 760 Torr

With 4-methyl-morpholine; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo0604890

Reference yield:

: 142-61-0
Hexanoyl chloride

: 22083-60-9,41955-14-0,116095-17-1,139066-86-7
antimycin A3

Guidance literature:: Multi-step reaction with 11 steps

1.1: 100 percent / Et₃N; LiCl / tetrahydrofuran / 16.5 h / 20 °C

2.1: TiCl₄; TMEDA / CH₂Cl₂ / 1 h / -20 °C

2.2: 90 percent / CH₂Cl₂ / 9 h / -20 - -5 °C

3.1: 89 percent / pyridine; DMAP / CH₂Cl₂ / 8 h / 0 °C

4.1: 74 percent / DMAP / CH₂Cl₂ / 46.5 h / 20 °C

5.1: 98 percent / NaIO₄ / tetrahydrofuran; H₂O / 3 h / cooling

6.1: 100 percent / N,N'-dicyclohexylcarbodiimide; DMAP / CH₂Cl₂ / 26 h / 20 °C

7.1: 100 percent / hydrogen / Pd(OH)2/C / methanol / 8 h / 40 °C / 22800 Torr

8.1: 62 percent / DMAP; 2-methyl-6-nitrobenzoic acid anhydride; molecular sieves 4 Angstroem / toluene / 16 h / 20 °C

9.1: 100 percent / trifluoroacetic acid / CH₂Cl₂ / 9.5 h / 20 °C

10.1: 94 percent / HOBt; EDC*HCl; N-methylmorpholine / dimethylformamide / 23 h / 30 °C

11.1: 100 percent / hydrogen / Pd/C / ethyl acetate / 6.5 h / 30 °C / 760 Torr

With 4-methyl-morpholine; pyridine; dmap; sodium periodate; N,N,N,N,-tetramethylethylenediamine; 4 A molecular sieve; 2-methyl-6-nitrobenzoic anhydride; hydrogen; titanium tetrachloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; lithium chloride; palladium dihydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo0604890