dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate

Base Information

Chemical Name:dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate
CAS No.:20473-57-8
Molecular Formula:C₁₆H₁₄N₂O₅
Molecular Weight:314.298
Hs Code.:

Synonyms:dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate

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Chemical Property of dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate

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Technology Process of dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate

There total 7 articles about dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 4518-10-9
Methyl 3-aminobenzoate

: 909780-30-9
C₁₆H₁₄N₂O₄

: 20473-57-8
dimethyl 3,3'-diazene oxide 1,2-diyldibenzoate

Guidance literature:: With selenium(IV) oxide; dihydrogen peroxide; In methanol; water; at 20 ℃; for 11h;
DOI:10.1055/s-2008-1067088

Reference yield: 86.0%

: 26960-97-4
methyl 3-nitrosobenzoate

: 20473-57-8
1,2-bis(3-(methoxycarbonyl)phenyl)diazene oxide

Guidance literature:: With cyclohexanone; In dimethyl sulfoxide; at 20 ℃; Catalytic behavior; Flow reactor;
DOI:10.1002/ejoc.202100006

Reference yield:

: 99769-19-4
[3-(methoxycarbonyl)phenyl]boronic acid

: 20473-57-8
1,2-bis(3-(methoxycarbonyl)phenyl)diazene oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydrogen bifluoride / methanol; water / 0.03 h / 0 - 20 °C / Inert atmosphere

1.2: 0.02 h / 20 °C

2.1: sodium tetrahydroborate; ammonium sulfate / ethanol / 0.5 h / 20 °C

With ammonium sulfate; sodium tetrahydroborate; potassium hydrogen bifluoride; In methanol; ethanol; water;
DOI:10.1021/jo300551m