3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

Base Information

Chemical Name:3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide
CAS No.:97163-51-4
Molecular Formula:C₁₃H₁₈N₃O₂S*I
Molecular Weight:407.275
Hs Code.:

Synonyms:3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

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Chemical Property of 3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

Chemical Property:

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Technology Process of 3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

There total 3 articles about 3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 97163-50-3
N-<4-<2-(1H-Imidazol-1-yl)ethyl>phenyl>methanesulfonamide

: 74-88-4
methyl iodide

: 97163-51-4
3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

Guidance literature:: In methanol; at 75 ℃; for 24h;
DOI:10.1021/jm00387a020

Reference yield:

: 56643-91-5
1-<2-(4-nitrophenyl)ethyl>-1H-imidazole

: 97163-51-4
3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethanol / 1 h / 2585.7 Torr / Ambient temperature

2: triethylamine / CH₂Cl₂ / 1.5 h / -10 - 20 °C

3: 48 percent / methanol / 24 h / 75 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1021/jm00387a020

Reference yield:

: 97163-49-0
1-[2-(4-aminophenyl)ethyl]-1H-imidazole

: 97163-51-4
3-methyl-1-<2-<4-<(methylsulfonyl)amino>phenyl>ethyl>-1H-imidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 1.5 h / -10 - 20 °C

2: 48 percent / methanol / 24 h / 75 °C

With triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm00387a020