(2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

Base Information

Chemical Name:(2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde
CAS No.:429675-57-0
Molecular Formula:C₃₀H₃₂O₅
Molecular Weight:472.581
Hs Code.:

Synonyms:(2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

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Chemical Property of (2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

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Technology Process of (2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

There total 6 articles about (2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 111085-83-7
1-(3,4,6-tri-O-benzyl-α-D-fructofuranosyl)-2-propene

: 429675-57-0
(2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

Guidance literature:: With acetic anhydride; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)02393-0

Reference yield:

: 429675-56-9
(2R,3R,4S,5S)-3,4-Bis-benzyloxy-2-benzyloxymethyl-8-iodomethyl-1,7-dioxa-spiro[4.4]nonane

: 429675-57-0
(2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Zn; AcOH / diethyl ether; ethanol / 24 h

2: DMSO; Ac₂O / 24 h

With acetic anhydride; acetic acid; dimethyl sulfoxide; zinc; In diethyl ether; ethanol;
DOI:10.1002/1521-3765(20020902)8:17<3976::AID-CHEM3976>3.0.CO;2-7

Reference yield:

: 100-39-0
benzyl bromide

: 429675-57-0
(2R,3S,4R,5R)-2-Allyl-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / NaH / dimethylformamide

2: 57 percent / boron trifluoride etherate

3: 98 percent / I₂ / tetrahydrofuran

4: 80 percent / Zn; AcOH / ethanol; diethyl ether

5: 83 percent / DMSO; Ac₂O

With iodine; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; zinc; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)02393-0