N²-(2,5-Di-tert-butylphenyl)-N¹-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid

Base Information

• Chemical Name: N²-(2,5-Di-tert-butylphenyl)-N¹-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid
• CAS No.: 118561-00-5
• Molecular Formula: C₄₀H₃₄N₂O₅
• Molecular Weight: 622.72

Synonyms:N²-(2,5-Di-tert-butylphenyl)-N¹-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid

Chemical Property of N²-(2,5-Di-tert-butylphenyl)-N¹-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid

Chemical Property:

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Technology Process of N²-(2,5-Di-tert-butylphenyl)-N¹-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid

There total 4 articles about N²-(2,5-Di-tert-butylphenyl)-N¹-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N2-(2,5-Di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid (130296-50-3) + 2-bromoethanol (540-51-2) → N2-(2,5-Di-tert-butylphenyl)-N1-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid (118561-00-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 24h;

DOI:10.1002/1521-3765(20021216)8:24<5630::AID-CHEM5630>3.0.CO;2-Z

Reference yield:

perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-carboxamide (33955-42-9) → N2-(2,5-Di-tert-butylphenyl)-N1-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid (118561-00-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / Zn(OAc)2 / quinoline / 2 h / 220 °C

2: 24 percent / K₂CO₃ / dimethylformamide / 24 h / 100 °C

With zinc diacetate; potassium carbonate; In quinoline; N,N-dimethyl-formamide;

Reference yield:

2,5-di-tert-butylaniline (21860-03-7) → N2-(2,5-Di-tert-butylphenyl)-N1-(2-hydroxyethyl)-3,4:9,10-perylentetracarboxdiimid (118561-00-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / Zn(OAc)2 / quinoline / 2 h / 220 °C

2: 24 percent / K₂CO₃ / dimethylformamide / 24 h / 100 °C

With zinc diacetate; potassium carbonate; In quinoline; N,N-dimethyl-formamide;

upstream raw materials:

N²-(2,5-Di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid

2-bromoethanol

perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-carboxamide

2,5-di-tert-butylaniline

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