C₃₆H₃₀N₄O₂

Base Information

• Chemical Name: C₃₆H₃₀N₄O₂
• CAS No.: 1448522-45-9
• Molecular Formula: C₃₆H₃₀N₄O₂
• Molecular Weight: 550.66
• Mol file: 1448522-45-9.mol

Synonyms:C₃₆H₃₀N₄O₂

Chemical Property of C₃₆H₃₀N₄O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₃₀N₄O₂

There total 5 articles about C₃₆H₃₀N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

C36H34N4O4 (1448522-54-0) → C36H30N4O2 (1448522-45-9)

Guidance literature:

With tetrachloromethane; triethylamine; triphenylphosphine; In acetonitrile; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol401812h

Reference yield:

2,3-dibromobenzene (583-53-9) → C36H30N4O2 (1448522-45-9)

Guidance literature:

Multi-step reaction with 4 steps

1: palladium diacetate; tri-tert-butyl phosphine; caesium carbonate / toluene / Inert atmosphere; Reflux

2: potassium hydroxide / methanol; water / 10 h / Inert atmosphere; Reflux

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / 5 - 20 °C / Inert atmosphere

4: triphenylphosphine; triethylamine; tetrachloromethane / acetonitrile / 20 °C / Inert atmosphere

With tetrachloromethane; tri-tert-butyl phosphine; palladium diacetate; benzotriazol-1-ol; caesium carbonate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; water; toluene; acetonitrile;

DOI:10.1021/ol401812h

Reference yield:

2-carbomethoxyaniline (134-20-3) → C36H30N4O2 (1448522-45-9)

Guidance literature:

Multi-step reaction with 4 steps

1: palladium diacetate; tri-tert-butyl phosphine; caesium carbonate / toluene / Inert atmosphere; Reflux

2: potassium hydroxide / methanol; water / 10 h / Inert atmosphere; Reflux

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / 5 - 20 °C / Inert atmosphere

4: triphenylphosphine; triethylamine; tetrachloromethane / acetonitrile / 20 °C / Inert atmosphere

With tetrachloromethane; tri-tert-butyl phosphine; palladium diacetate; benzotriazol-1-ol; caesium carbonate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; water; toluene; acetonitrile;

DOI:10.1021/ol401812h

upstream raw materials:

2,3-dibromobenzene

2-carbomethoxyaniline

C₂₂H₂₀N₂O₄

o-phenylenedianthranilic acid